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and highly reusable organoalysts for the asymmetric direct aldol reaction of benzaldehydes developing new robust, efficient and recyclable organoalysts procedure.5 Two different lengths of the bromoalkyl chain (n = 1 and 4) .. ball-mill: 9a (89 mg, 0.59 mmol), 10a (67 L, 0.65 mmol), 1b (40 mg, .....

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Aldol reaction / Asymmetric organocatalysis / Water / Solvent-free reactions / Prolinethioamidesreaction times and result in simple and efficient workup procedures.[9] Forbecome a highly pursued goal in green chemistry.efficacy of catalystd was similar when the reaction was performed in a ball mill[9a,9b] (Table,....

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The reaction was catalyzed by the methyl ester of (S)-proline-(S)-phenylalanine, (S,S)-1a (7 mol %) and proceed efficiently affording the anti-aldol products in high yields and with good diastereoand enantioselectivities (up to 91:9 dr, up to 95% ee). 16,17 We could demonstrate that dipeptide (S,S)-1a was more efficient organocatalyst in the asymmetric aldol reaction under solvent-free conditions, relative to the same reaction in solution....

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